| 固相萃取-液相色谱-串联质谱法测定婴幼儿乳粉中乙基麦芽酚 |
| |
| 引用本文： | 杨东东,李实飞,林正锋,谢文强,杨雪莲,王朝政. 固相萃取-液相色谱-串联质谱法测定婴幼儿乳粉中乙基麦芽酚[J]. 中国乳品工业, 2022, 0(1): 48-51 |
| |
| 作者姓名： | 杨东东 李实飞 林正锋 谢文强 杨雪莲 王朝政 |
| |
| 作者单位： | 海口海关技术中心;北京工商大学食品添加剂与配料北京高校工程研究中心;海南大学食品学院 |
| |
| 基金项目： | 海南省自然科学基金青年基金项目(218QN327)。 |
| |
| 摘 要： | 建立了固相萃取柱-液相色谱-串联质谱法检测婴幼儿乳粉中乙基麦芽酚的方法.样品采用水-叔丁基甲醚提取,氢氧化钠溶液反萃后经溶剂蒸发工作站除去微量叔丁基甲醚,用HLB固相萃取柱实现净化及浓缩.该方法在2～100 ng/mL质量浓度范围内线性关系良好,相关系数达0.999,测定低限可达2.0 μg/kg,乳粉样品在5,10,...
|
| 关 键 词： | 婴幼儿配方乳粉 乙基麦芽酚 固相萃取 液相色谱-串联质谱法 |
Determination of Ethyl Maltol in Infant Formula Milk Powder by Ultra High Performance Liquid Chromatography-Tandem Mass Spectrometry with Solid Phase Extraction |
| |
| YANG Dongdong,LI Shifei,LIN Zhengfeng,XIE Wenqiang,YANG Xuelian,WANG Chaozheng. Determination of Ethyl Maltol in Infant Formula Milk Powder by Ultra High Performance Liquid Chromatography-Tandem Mass Spectrometry with Solid Phase Extraction[J]. China Dairy Industry, 2022, 0(1): 48-51 |
| |
| Authors: | YANG Dongdong LI Shifei LIN Zhengfeng XIE Wenqiang YANG Xuelian WANG Chaozheng |
| |
| Affiliation: | (Technology Center of Haikou Customs District,Haikou 570311,China;Beijing Higher Institution Engineering Research Center of Food Additives and Ingredients,Beijing Technology&Business University(BTBU),Beijing 100048,China;College of Food Science and Technology,Hainan University,Haikou 570228,China) |
| |
| Abstract: | An analytical method based on solid phase extraction high-performance liquid chromatography-tandem mass spectrometry(HPLC-MS/MS)was developed for detecting ethyl maltol in infant formula milk powder.The samples were extracted by water and tert butyl methyl ether,and the supernatant was extraction by alkali solution(pH>13).After evaporation for removing trace MTBE,the solvent wascleaned up and concentrated on a HLB column.The results showed that the method had a good linearity range between 2.0~100 ng/mL(R2=0.999)and the detection limit was as low as 2.0μg/kg.The recoveries of ethyl maltol range from 71.2%to 110.4%at spiked levels of 5,10,20,50 and 100μg/kg,and relative standard deviations range from 6.2%to 9.8%(n=6).The method is sensitive,accurate and reliable. |
| |
| Keywords: | infant formula milk powder ethyl maltol solid phase extraction ultra high performance liquid chromatography-tandem mass spectrometry |
| 本文献已被 维普 等数据库收录！ |
|
