| 毛细管气相色谱法测定饮料中苯甲醛 |
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| 引用本文： | 王建刚.毛细管气相色谱法测定饮料中苯甲醛[J].吉林化工学院学报,2008,25(4):8-9. |
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| 作者姓名： | 王建刚 |
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| 作者单位： | 吉林化工学院分析测试中心,吉林,吉林,132022 |
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| 摘 要： | 建立了毛细管气相色谱测定饮料中苯甲醛含量的方法．采用PEG-20M（30m×0．32mm×0．25μm）色谱柱，程序升温，FID检测器检测．结果苯甲醛在50μg·mL^～1-800μg·mL^-1范围内，色谱峰面积与浓度成线性关系，相关系数0．9991，平均回收率95．2％，相对标准偏差4．5％，方法检出限5μg·g^-1．本方法简单、准确，适合饮料中苯甲醛含量测定．
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| 关 键 词： | 气相色谱 苯甲醛 饮料 |
Determination of benzaldehyde by gas chromatography |
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| WANG Jian-gang.Determination of benzaldehyde by gas chromatography[J].Journal of Jilin Institute of Chemical Technology,2008,25(4):8-9. |
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| Authors: | WANG Jian-gang |
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| Affiliation: | WANG Jian-gang ( Center of Analysis and Measurement, Jilin Institute of Chemical Technology, Jilin 132022, China) |
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| Abstract: | Benzaldehyde in drinks was determined by Gas Chromatography with FID after complete separation with PEG-20M(30m×0.32m×0.25m) capillary column.The good linearity between peak area and concentration was obtained within the range of 50g/mL to 800g/ml(R=0.997).The lowest detectable limit was 5μg·g-1.The average recovery rate was 95.2%(RSD=2.4%).The procedure is simple,accurate and reproducible,and suitable for quality control of drinks. |
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| Keywords: | Gas chromatography benzaldehyde drinks |
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