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MBS树脂合成技术的中试研究(Ⅲ)MBS胶乳的凝聚
引用本文:黄金霞,李晶,吴辉,赵金德,张会轩. MBS树脂合成技术的中试研究(Ⅲ)MBS胶乳的凝聚[J]. 弹性体, 2006, 16(6): 17-20
作者姓名:黄金霞  李晶  吴辉  赵金德  张会轩
作者单位:1. 长春工业大学,吉林,长春,130022;吉化集团精细化工技术中心,吉林,吉林,132021
2. 吉化集团精细化工技术中心,吉林,吉林,132021
3. 长春工业大学,吉林,长春,130022
摘    要:阐述了聚合物乳液的凝聚机理和MBS接枝胶乳的凝聚工艺,在MBS胶乳凝聚小试研究和MBS接枝胶乳中试研究的基础上进行了MBS接枝胶乳凝聚的中试研究,着重研究了凝聚剂种类、用量和加料方式以及凝聚温度、水胶比等对MBS粉料堆密度和粒度分布的影响,确定了MBS胶乳的凝聚工艺,为5 000 t/a MBS树脂生产装置提供了设计依据.

关 键 词:MBS胶乳  凝聚机理  凝聚工艺  凝聚剂  堆密度  中试
文章编号:1005-3174(2006)06-0017-04
修稿时间:2006-05-25

Research on pilotscale synthesis of MBS resin(Ⅲ)Coagulation of MBS latex
HUANG Jin-xia,LI Jing,WU Hui,ZHAO Jin-de,ZHANG Hui-xuan. Research on pilotscale synthesis of MBS resin(Ⅲ)Coagulation of MBS latex[J]. China Elastomerics, 2006, 16(6): 17-20
Authors:HUANG Jin-xia  LI Jing  WU Hui  ZHAO Jin-de  ZHANG Hui-xuan
Abstract:The coagulation mechanism of polymer latex and the coagulation process of MBS grafting latex were reviewed firstly;pilotscale experiments of coagulation of MBS latex were carried out basing on the process of small scale experiment of coagulation of MBS latex and pilotscale experiment results of synthesis of SBR latex and synthesis of MSB latex.The effects of the type and amount of coagulant,charging sequence,coagulation temperature and the ratio of amount of coagulant aqueous solution to the amount of MBS latex on bulk density and particle size distribution of MBS powder were investigated experimentally,and the coagulation process of MBS latex was concluded.These results provided a basis for the design of 5000t/a MBS plant.
Keywords:MBS latex  coagulation mechanism  coagulation process  coagulant  bulk density  pilotscale experiment
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