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(Y,Eu)2O3红生粉的粒度和形貌控制研究
引用本文:赖华生,王林生,文小强,周新华,袁德林,周健.(Y,Eu)2O3红生粉的粒度和形貌控制研究[J].江西有色金属,2009,23(2):23-25.
作者姓名:赖华生  王林生  文小强  周新华  袁德林  周健
作者单位:赣州有色冶金研究所,江西赣州341000
摘    要:以草酸共沉淀法制备(Y,Eu)2O3为红生粉,对比六种沉淀方式对红生粉形貌的影响,其中在沉淀过程中添加氨水并用双加料的方式可制备出形貌上优于红生粉商品,其粒度分布呈正态分布;通过调节草酸过量系数、沉淀过程中添加氨水的量、合成温度及草酸浓度等沉淀条件可控制红生粉D50的变化。

关 键 词:(Y  Eu)2O3  形貌  粒度

On Morphology and Partical Size Conrol of (Y,Eu)2O3 Precursor
Affiliation:LAI Hua-sheng, WANG Lin-sheng, WEN Xiao-qiang, ZHOU Xin-hua, YUAN De-lin, ZHOU Jia (Ganzhou Nonferrous Metallurgy Research Institute, Ganzhou 341000, Jiangxi, China)
Abstract:The(Y,Eu)2O3 Precursor which is superior to commercial one on morphology was prepared by precipitation method of oxalic acid. The effect of reaction conditions on morphology and particle size of (Y,Eu)2O3 precursor was investigated. The results show the medium particle size of precursor was influenced mainly by these facts: concentration of rare earth solution, excessive amount of oxalic acid, concentration of ammonia, concentration of oxalic acid and temperature of reaction.
Keywords:(Y  Eu)2O3  morphology  particle size
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