| GC-MS/MS法测定葡萄酒中的苯类添加剂 |
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| 引用本文： | 田玉平,王东辉,王虎.GC-MS/MS法测定葡萄酒中的苯类添加剂[J].化学世界,2011,52(4):211-215. |
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| 作者姓名： | 田玉平 王东辉 王虎 |
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| 作者单位： | 上海市计量测试技术研究院,上海,201203 |
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| 基金项目： | 上海市科学技术委员会资助(10142201100) |
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| 摘 要： | 利用气相色谱串联质谱(GC-MS/MS)法测定葡萄酒中苯类添加剂:苯甲酸、叔丁基对苯二酚、2,6-二叔丁基-4-甲基苯酚、对羟基苯甲酸正丁酯.试样经乙酸乙酯超声波提取葡萄酒中的上述几种苯类添加剂,经过对苯甲酸、叔丁基对苯二酚等多反应监测(MRM)扫描离子对的选择,并对串联质谱的各参数进行优化.方法检测限为:苯甲酸0.0...
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| 关 键 词： | GC-MS/MS 苯类添加剂 葡萄酒 |
Simultaneous Testing Additives in Wine by GC-MS/MS |
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| TIAN Yu-ping,WANG Dong-hui,WANG Hu.Simultaneous Testing Additives in Wine by GC-MS/MS[J].Chemical World,2011,52(4):211-215. |
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| Authors: | TIAN Yu-ping WANG Dong-hui WANG Hu |
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| Affiliation: | TIAN Yu-ping,WANG Dong-hui,WANG Hu(Shanghai Institute of Measurement and Testing Technology,Shanghai 201203,China) |
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| Abstract: | A method was established for simultaneous determination of additives in wine,including benzoic acid,tert-butylhydroquinone,2,6-di-tertbutyl-4-methylophenol,butylparaben by GC-MS/MS.The sample was extracted by ethyl acetate, cleaned up,and then determinted with GC-MS/MS.When the target compounds' concentration were at 0.05,0.5,1.0 μg/mL level,the precision was 4.5%~8.1%,the recovery was at the range of 88.4%~115.7%,the LOD was at 10-8 level.The method meets the requirements of our country,and has been applied to real sample analysis. |
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| Keywords: | GC-MS/MS additives wine |
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