| 固定床电化学反应器内电化学氧化法制备2,5-二甲氧基二氢呋喃 |
| |
| 引用本文： | 许文林,王雅琼. 固定床电化学反应器内电化学氧化法制备2,5-二甲氧基二氢呋喃[J]. 化学反应工程与工艺, 2001, 17(2): 185-188 |
| |
| 作者姓名： | 许文林 王雅琼 |
| |
| 作者单位： | 扬州大学理学院化学化工系, |
| |
| 基金项目： | 江苏省普通高等学校“青蓝工程”跨世纪学术带头人基金资助 |
| |
| 摘 要： | 固定床电化学反应器内间接电化学氧化呋喃制备2，5－二甲氧基二氢呋喃的过程进行了研究，确定了电解条件及产品的分离与提纯工艺，研究表明，在操作温度为0－5℃的反应系统中，操作槽电压为4．0－6．0V，反应表观电流密度≥2000A／m^2，产品收率≥90％，电流效率≥90％，能耗（直流电）≤3．0kwh/kg产品。
|
| 关 键 词： | 固定床 电化学氧化 2 5－二甲氧基二氢呋喃 制备 电化学反应器 |
| 文章编号： | 1001－7631（2001）02－0185－04 |
| 修稿时间： | 2000-06-20 |
INDIRECT ELECTROCHEMICAL PREPARATION OF 2,5-DIMETHOXY-2,5-DIHYDROFURAN FROM FURAN IN A PACKED BED ELECTROCHEMICAL REACTOR |
| |
| XU Wen-lin,WANG Ya-qiong. INDIRECT ELECTROCHEMICAL PREPARATION OF 2,5-DIMETHOXY-2,5-DIHYDROFURAN FROM FURAN IN A PACKED BED ELECTROCHEMICAL REACTOR[J]. Chemical Reaction Engineering and Technology, 2001, 17(2): 185-188 |
| |
| Authors: | XU Wen-lin WANG Ya-qiong |
| |
| Abstract: | An indirect electrochemical preparation of 2,5-dimethoxy-2,5-dihydrofuran from furan in a packed bed electrochemical reactor was described. The experimental results showed that the current efficiency was more than 90%, the product yield was more than 90% and the electric energy consumption was less than 3.0kwh／kg product under the optimized operating conditions such as 0℃～5℃ reaction temperature, 4.0V～ 6.0V electrolysis voltage and more than 2000A/m2 operating current density. |
| |
| Keywords: | packed bed electrochemical oxidation 2 5 dimethoxy 2 5 dihydrofuran |
| 本文献已被 CNKI 维普 万方数据 等数据库收录！ |
