| 十二醇/三聚氰胺-甲醛核壳结构材料的制备 |
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| 引用本文： | 余丽蓉,陆春华,高树军,许仲梓. 十二醇/三聚氰胺-甲醛核壳结构材料的制备[J]. 陶瓷科学与艺术, 2007, 0(2) |
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| 作者姓名： | 余丽蓉 陆春华 高树军 许仲梓 |
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| 作者单位： | 南京工业大学材料科学与工程学院 江苏南京210009 |
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| 基金项目： | 教育部跨世纪优秀人才资助项目 |
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| 摘 要： | 采用原位聚合法以三聚氰胺-甲醛树脂为壁材、十二醇为芯材,合成了十二醇/三聚氰胺-甲醛核壳结构材料.研究了复相乳液形成区、反应物摩尔比及反应条件对合成的影响,确定了合适的反应工艺,并利用红外光谱仪、扫描电子显微镜、热失重分析仪及激光粒度分析仪对产物进行红外特征吸收光谱、表面形态、粒径分布以及热质量损失情况的分析。结果表明,该材料具有良好的外观特性及热稳定性,可用于特种涂料的制备。
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| 关 键 词： | 原位聚合 相变复合核壳结构材料 十二醇 三聚氰胺-甲醛树脂 |
Synthesis of dodecanol/melamine-formaldehyde resin with core-shell structure |
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| YU Li-rong,LU Chun-hua,GAO Shu-jun,XU Zhongzi. Synthesis of dodecanol/melamine-formaldehyde resin with core-shell structure[J]. Ceramics Science & Art, 2007, 0(2) |
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| Authors: | YU Li-rong LU Chun-hua GAO Shu-jun XU Zhongzi |
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| Abstract: | The phase change composite core-shell structure material was synthesized via in situ polymerization by using melamine-formaldehyde resin as wall material and dodecanol as core materials.The sample preparation technology was studied and the appropriate reaction conditions were obtained.IR,SEM,the particle size distributions and TG of samples were tested.The results indicated that the new material has good a quality which was suitable for special coating. |
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| Keywords: | in saitu polymerization core-shell structure material dodecanol melamine-formaldehyde resin |
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