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常温下高氯酸-冰醋酸混合液制取渗金属薄膜样品
引用本文:李巧玲,叶云. 常温下高氯酸-冰醋酸混合液制取渗金属薄膜样品[J]. 分析测试仪器通讯, 1996, 0(2)
作者姓名:李巧玲  叶云
作者单位:华北工学院
摘    要:使用046mol/LHClO4167mol/LHAc电解抛光溶液进行实验,确定了常温下制取渗金属薄膜样品的电解抛光参数,为Bolmann法制取电镜用薄膜样品提供了电解参数选择方法。

关 键 词:薄膜样品  抛光参数

Preparation of Osmotic Metal Film Sample with Perchloric Acid and Glacial Acetic Acid at Atmospheric Temperature
Li Qiaoling,Ye Yun. Preparation of Osmotic Metal Film Sample with Perchloric Acid and Glacial Acetic Acid at Atmospheric Temperature[J]. , 1996, 0(2)
Authors:Li Qiaoling  Ye Yun
Abstract:A study on electrolytic polishing parameter for preparation of osmatic metal film sample in electrolytic polishing liquid of 0.46 mol/L HClO 4 1.67 mol/L HAc at atmospheric temperature was reported in this paper. And method for election of electrolytic parameters in preparing electron microscope film samples with Bollmann means was also provided.
Keywords:electron microscope film sample   polishing parameter  
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