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Fe-Ce-Ni纳米晶粉体的机械合金化研究
引用本文:曹奇志,欧阳义芳,张晶,李建映,黄自谦. Fe-Ce-Ni纳米晶粉体的机械合金化研究[J]. 中国粉体技术, 2011, 17(3). DOI: 10.3969/j.issn.1008-5548.2011.03.015
作者姓名:曹奇志  欧阳义芳  张晶  李建映  黄自谦
作者单位:1. 广西师范学院物理与电子信息科学系,广西南宁,530023
2. 广西大学物理学院,广西南宁,530004
基金项目:感谢广西师范学院青年基金
摘    要:研究按物质的量配比分别为n(Fe-Ce)∶n(Ni)=0.7∶0.3和n(Fe-Ni)∶n(Ce)=0.8∶0.2的混合粉体在机械合金化过程中的结构演变和软磁性,采用X射线衍射法表征机械合金化粉体的结构演变过程,用振动样品磁强计对样品的静磁性能进行测试分析。结果表明:球磨150 h后,按物质的量配比为n(Fe-Ce)∶n(Ni)=0.7∶0.3和n(Fe-Ni)∶n(Ce)=0.8∶0.2的混合粉体都分别成为纳米晶粉体,球磨时间和Ni成分的含量都对其软磁性能有影响。

关 键 词:机械合金化  纳米晶  软磁性

Fe-Al-Ni Nano-crystalline Powders Prepared by Mechanical Alloy
Cao Qizhi,Ouyang Yifang,Zhang Jing,Li Jianying,Huang Ziqian. Fe-Al-Ni Nano-crystalline Powders Prepared by Mechanical Alloy[J]. China Powder Science and Technology, 2011, 17(3). DOI: 10.3969/j.issn.1008-5548.2011.03.015
Authors:Cao Qizhi  Ouyang Yifang  Zhang Jing  Li Jianying  Huang Ziqian
Abstract:The structural evolution and soft magnetism of the elemental powders in molar ratio of n(Fe-Ce)∶ n(Ni) =0.7∶ 0.3 and n(Fe-Ni)∶ n(Ce)=0.8∶0.2 respectively were researched by mechanical alloying method.The structural evolution was characterized by X-ray diffraction(XRD) and the soft magnetism was measured by vibrating sample magnetometer(VSM).The experimental results showed that the last milling products of the elemental powders in molar ratio of n(Fe-Ce)∶ n(Ni) =0.7∶0.3 and n(Fe-Ni)∶n(Ce)=0.8∶0.2 respectively were nanocrystalline.The soft magnetic properties of the samples were affected by the milling time and Ni content of the powders.
Keywords:mechanical alloying  nano-crystalline  soft magnetism
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