| 9,9-双(羟甲基)芴的合成工艺研究 |
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| 引用本文： | 杜焰,谢昌琮,廖维林. 9,9-双(羟甲基)芴的合成工艺研究[J]. 化工技术与开发, 2003, 32(5): 4-5,26 |
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| 作者姓名： | 杜焰 谢昌琮 廖维林 |
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| 作者单位： | 1. 江西师范大学化学学院,江西,南昌,330027
2. 江西省医药设计院,江西,南昌,330046 |
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| 摘 要： | 以芴为原料，经甲醛羟甲基化反应合成了新型给电子体1，3-双醚的前体，总收率达65％，并对生产工艺进行了优化研究。
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| 关 键 词： | 9，9-双（羟甲基）芴 合成工艺 芴 甲醛 羟甲基化 催化剂 生产方法 |
| 文章编号： | 1671-9905(2003)05-0004-02 |
Research on Synthesis of 9,9-Bis(hydromethyl) Fluorene |
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| DU Yan,XIE Cheng-cong,LIAO Wei-lin. Research on Synthesis of 9,9-Bis(hydromethyl) Fluorene[J]. Technology & Development of Chemical Industry, 2003, 32(5): 4-5,26 |
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| Authors: | DU Yan XIE Cheng-cong LIAO Wei-lin |
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| Affiliation: | DU Yan~1,XIE Cheng-cong~2,LIAO Wei-lin~1 |
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| Abstract: | Used sodium ethoxide/alcohol solution as catalyst and 1,3-disther as material, 9,9-bis(hydromethyl) fluorene was synthesized through method of hydromethylation. The influence factors of yield were discussed. The optimum reaction processes were studied. |
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| Keywords: | bis(hydromethyl)fluorine hydromethylation 1 3-diether |
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