| 六氢化邻苯二甲酸二异丁酯合成中的催化加氢 |
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| 引用本文： | 商红岩,韩哲茵,姜翠玉,张晓云,江少明. 六氢化邻苯二甲酸二异丁酯合成中的催化加氢[J]. 石油化工, 1999, 28(7): 462-465 |
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| 作者姓名： | 商红岩 韩哲茵 姜翠玉 张晓云 江少明 |
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| 作者单位： | 石油大学炼制系,山东省东营,257062 |
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| 摘 要： | 研究了反应氢气压力、反应温度、反应介质（ｐＨ）以及催化剂对四氢化邻苯二甲酸体系和四氢化邻苯二甲酸二异丁酯体系加氢效果的影响。通过对比研究，确定了合成六氢化邻苯二甲酸二异丁酯（ＤＩＢＥ）的先酯化后加氢的合成路线、最佳合成条件及选择性加氢催化剂
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| 关 键 词： | 酯化 催化剂 氢化 顺丁烯二酸酐 |
| 修稿时间： | 1998－07－11 |
The Study of Hydrogenation in the Synthesis of Di-Isobutyl Hexahydrophthalate |
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| SHANG Hong-yan,HAN Zhe-yin,JIANG Cui-yu,ZHANG Xiao-yun,JIANG Shao-ming. The Study of Hydrogenation in the Synthesis of Di-Isobutyl Hexahydrophthalate[J]. Petrochemical Technology, 1999, 28(7): 462-465 |
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| Authors: | SHANG Hong-yan HAN Zhe-yin JIANG Cui-yu ZHANG Xiao-yun JIANG Shao-ming |
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| Abstract: | In this paper,we studied the influences of hydrogen pressure,temperature,reaction medium(or pH value)and catalysts on hydrogenation of tetrahydrophthalic acid and di-isobutyl tetrahydrophthalate.On the basis of experimental results,a suitable route for the synthesis of di-isobutyl hexahydrophthalate is established including the most appropriate reaction conditions,catalysts of high activity and high selectivity to alkenyl double bond. |
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| Keywords: | esterification catalyst hydrogenation maleic anhydride |
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