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Supramolecular-templated synthesis of mesoporous silica-zirconia nanocomposite
Authors:FANG Hua  LIU Rui-tang  SHI Wei-hai  MA Chun-yang
Abstract:Mesoporous SiO_2-ZrO_2 nanocomposite was successfully prepared by using supramolecular triblock copolymer as the template through evaporation-induced self-assembly approach. The textural and structural properties were characterized by X-ray diffraction, nitrogen adsorption analysis, and transmission electron microscope. Comparison between pure mesoporous silica and mesoporous silica-zirconia nanocomposite was also presented in this work. The surface area, pore size, and pore volume decreased as the Zr doping in the mesoporous silica framework. But the obtained nanocomposite maintained the cubic Im3m-type mesoporous structure.
Keywords:silica  zirconia  mesoporous composite  evaporation-induced self-assembly
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