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工业盐酸中微量氟的测定
引用本文:李永波. 工业盐酸中微量氟的测定[J]. 福建分析测试, 2002, 11(3): 1605,1621
作者姓名:李永波
作者单位:福建省测试技术研究所,福建,福州,350003
摘    要:样品分离氯离子后,在弱酸性介质中,用氟离子选择性电极、已知量添加法测定工业盐酸中微量氟。本方法标准偏差为5×10~(-5)%,变异系数<6%。回收率在91.8~104.0%。方法简便、数据准确。

关 键 词:盐酸    氟离子选择性电极  增量法

Determinaton of trace fluorion in hydrochloric acid by fluorion ISE
Li Yongbo. Determinaton of trace fluorion in hydrochloric acid by fluorion ISE[J]. Fujian Anal Ysis & Testing, 2002, 11(3): 1605,1621
Authors:Li Yongbo
Abstract:A rapid and simple method for the test of trace F in hydrochloric acid using F~--ISE, removing CL~- by AgNO_3 was presented.The slope of the electrode was 58.0mV.The suitable pH value was 5, and the Nernst Linear range was 0.5~5×10~(-5)M.The standard deviation was 5×10~(-5)%, the CV<6%, and the recovery was 91.8%~104.0%.
Keywords:Hydrochloric acid  Fluorine  F~- -ISE  Method of increment
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