Hydrothermal synthesis and characterization of a copper(I) halide coordination polymer with isonicotinic acid (IN) ligand as a template possessing three-dimensional supramolecular network structure |
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| Affiliation: | 1. Department of Chemistry, College of Chemistry and State Key Laboratory of Inorganic Synthesis and Preparative Chemistry, Jilin University, Changchun, 130023 Jilin, People''s Republic of China;2. Key Laboratory of Supramolecular Structure and Materials of Ministry of Education, Jilin University, Changchun, 130023 Jilin, People''s Republic of China;3. Department of Chemistry, Inner Mongolia University for Nationalities, People''s Republic of China;1. Institute for Solid State Research, IFW Dresden, Helmholtzstrasse 20, D-01069 Dresden, Germany;2. Ruđer Bošković Institute, Bijenička cesta 54, 10000 Zagreb, Croatia;3. University of Zurich, Rämistrasse 71, CH-8006 Zürich, Switzerland;4. Institute for Solid State Physics, Technical University Dresden, D-01062 Dresden, Germany;1. School of Chemistry, Monash University, Clayton, VIC 3800, Australia;2. Department of Microbiology, Monash University, Clayton, VIC 3800, Australia;1. Stefan S Nicolau Institute of Virology, Romanian Academy, Bucharest, Romania;2. Faculty of Chemistry, University of Bucharest, Romania;3. Institute of Cardiovascular Diseases Prof. Dr. C.C. Iliescu, Microbiology Department, Bucharest, Romania;4. University of Orleans, ICOA-UMR7311, CNRS, France |
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| Abstract: | The title compound [CuBr(IN)]n 1 was hydrothermally synthesized from a simple reaction of CuBr2–IN–KBr–NaOH–H2O. X-ray analysis revealed that it is a new example containing extended one-dimensional staircase chain in copper(I) halide family. Its structure can be better described as a three-dimensional supramolecular network assembled via a combination of coordinate–covalent bonds and intermolecular hydrogen bonds. Moreover, compound 1 was characterized by elemental analysis, IR spectrum and TGA analysis. |
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