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喷射电沉积镍枝晶基础工艺研究
引用本文:初晓辉,田宗军,黄因慧,刘志东,陈劲松,王桂峰.喷射电沉积镍枝晶基础工艺研究[J].电镀与精饰,2008,30(3):9-12.
作者姓名:初晓辉  田宗军  黄因慧  刘志东  陈劲松  王桂峰
作者单位:南京航空航天大学,机电学院,江苏,南京,210016
基金项目:国家自然科学基金资助项目(50575104)
摘    要:利用喷射电沉积工艺制备镍枝晶。试验在大电流脉冲电源作用下,通过改变溶液流量、电流、沉积时间、喷嘴与阴极距离,观察沉积物形态,研究各个参数对电沉积的影响。结果表明,随着溶液流量变大,阴极上长高的枝状晶根数变少,宏观上更疏松;随着电流增大,沉积形貌由圆柱体逐渐向倒圆锥过渡;沉积速度开始较慢,逐渐增加,最后保持稳定;喷嘴与阴极距离都对沉积物形态产生明显影响,试验测出了一个中间距离,在这个距离附近,沉积形状最接近圆柱。

关 键 词:喷射电沉积  枝晶    电流
文章编号:1001-3849(2008)03-0009-04
修稿时间:2007年6月1日

Research on Jet Electrodepositing Ni Dendritic Crystal
CHU Xiao-hui,TIAN Zong-jun,HUANG Yin-hui,LIU Zhi-dong,CHEN Jin-song,WANG Gui-feng.Research on Jet Electrodepositing Ni Dendritic Crystal[J].Plating & Finishing,2008,30(3):9-12.
Authors:CHU Xiao-hui  TIAN Zong-jun  HUANG Yin-hui  LIU Zhi-dong  CHEN Jin-song  WANG Gui-feng
Abstract:Dendritic crystals were made by jet electrodeposition.The experiment results show that the number of grown branches decreases and the appearance looks looser with the increase of liquor flux;the morphology of the deposits changed from cylinder to reversed cone with the increase of current;the reaction speed at the beginning is slow,and then added up slowly to a steady state;the distance of sprayer to the plate electrode has influence to the deposits,it was observed that the distance has a middle value under which the morphology of crystals was cylinder.
Keywords:jet electrodeposition  dendritic crystal  Ni  current
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