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金相试样制备技巧及具体方法
引用本文:谷秀锐,孙江欢,罗扬,张鹏,王佩. 金相试样制备技巧及具体方法[J]. 理化检验(物理分册), 2021, 57(1): 5-7,14
作者姓名:谷秀锐  孙江欢  罗扬  张鹏  王佩
作者单位:河钢集团钢研总院,石家庄050000
摘    要:合理的金相试样制备方法是获得清晰、高质量显微组织图像的保障,是材料金相研究的基础.对高纯钨、高氮不锈钢、汽车钢板、涂层材料的金相制备技巧及具体方法进行了分析,解决了制样中切割、镶嵌、磨抛和浸蚀等过程遇到的问题.结果表明:高纯钨硬度高,要保证磨抛时间;高氮不锈钢采用三氯化铁盐酸甘油混合液浸蚀,可获得浸蚀均匀的显微组织形貌...

关 键 词:金相试样  制备方法  高纯钨  高氮不锈钢  涂层材料

Preparation Techniques and Specific Methods of Metallographic Sample
GU Xiurui,SUN Jianghuan,LUO Yang,ZHANG Peng,WANG Pei. Preparation Techniques and Specific Methods of Metallographic Sample[J]. Physical Testing and Chemical Analysis Part A:Physical Testing, 2021, 57(1): 5-7,14
Authors:GU Xiurui  SUN Jianghuan  LUO Yang  ZHANG Peng  WANG Pei
Affiliation:(Steel Research Institute of HBIS,Shijiazhuang 050000,China)
Abstract:Reasonable metallographic sample preparation method is the guarantee to obtain clear and high quality microstructure image,and is the basis of metallographic study of materials.The metallographic preparation techniques and specific methods of high purity tungsten,high nitrogen stainless steel,automobile steel plate and coating material were analyzed,and the problems encountered in the process of cutting,inlaying,grinding and polishing and etching in sample preparation were solved.The results show that the hardness of high purity tungsten is high,so grinding and polishing time should be ensured.High nitrogen stainless steel agent can obtain uniform microstructure by etching with ferric chloride and glycerin hydrochloride mixture.The sample preparation of automobile steel plate should ensure that the sample is upright and not inclined,and avoid scratches during polishing.During the cutting,inlaying and grinding and polishing process of coating material sample preparation,the protective work should be done to ensure the integrity of coating.
Keywords:metallographic sample  preparation method  high purity tungsten  high nitrogen stainless steel  coating material
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