| 两种对甲氧基苄基腺嘌呤类化合物的合成及表征 |
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| 引用本文： | 孙文阳,梁镇海,韩灵翠.两种对甲氧基苄基腺嘌呤类化合物的合成及表征[J].现代化工,2009,29(Z1). |
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| 作者姓名： | 孙文阳 梁镇海 韩灵翠 |
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| 作者单位： | 太原理工大学化学化工学院,山西,太原,030024 |
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| 基金项目： | 山西省农社科技攻关资助项目 |
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| 摘 要： | 以对甲酚为原料,经对甲苯甲醚、对甲氧基苄基溴,再与腺嘌呤缩合,合成了N~6,N~9-二(对甲氧基苄基)腺嘌呤和N~6,N~6,N~9-三(对甲氧基苄基)腺嘌呤,利用红外光谱、核磁共振和质谱等检测手段对化合物的结构进行了表征,用萝卜子叶增重法测定了化合物的细胞分裂索活性,证明了2种对甲氧基苄基腺嘌呤类化合物都具有生物活性.
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| 关 键 词： | N~9-二(对甲氧基苄基)腺嘌呤 N~9-三(对甲氧基苄基)腺嘌呤 腺嘌呤 对甲氧基苄基溴 |
Synthesis and characterization of two kinds of P-methoxybenzyl adenine derivatives |
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| SUN Wen-yang,HANG Zhen-hai,HAN Ling-cui.Synthesis and characterization of two kinds of P-methoxybenzyl adenine derivatives[J].Modern Chemical Industry,2009,29(Z1). |
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| Authors: | SUN Wen-yang HANG Zhen-hai HAN Ling-cui |
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| Abstract: | Two new compounds,N~6,N~9-di(p-methoxybenzyl)adenine and,N~6,N~9,N~9-tri(p-methoxybenzyl)adenine,are synthesized by three steps of reactions as follows:from 4-methoxytoluene to 4-methylanisole,then to 4-methoxybenzyl bromide,and finally the prepared product condense with adenine.Their structures are characterized by IR,1H-NMR and MS,their activities of eytokinina are determined with radish cotyledons weight adding method,and the results prove that P-methoxybenzyl adenine derivatives have bioactivities. |
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| Keywords: | N~6 N~6 N~6 N~6 N~9-di(p-methoxybenzyl)adenine N~6 N~9 N~9-tri(p-methoxybenzyl)adenine adenine Pbromomethylanisole |
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