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菠萝酯的合成研究
引用本文:张剑红,田春良.菠萝酯的合成研究[J].化学工程师,2004,18(8):10-12.
作者姓名:张剑红  田春良
作者单位:临沂师范学院,附中,山东,临沂,276005;济宁师范专科学校,化学系,山东,济宁,272125
摘    要:以苯酚和氯乙酸为原料,四丁基碘化铵为催化剂合成了苯氧乙酸,收率达96.2%。并以苯氧乙酸和烯丙醇为原料,强酸性阳离子交换树脂为催化剂合成了菠萝酯,收率达84.5%。考察了两个反应的主要影响因素。

关 键 词:苯氧乙酸  烯丙醇  合成  菠萝酯
文章编号:1002-1124(2004)08-0010-03
修稿时间:2004年5月20日

Synthesis of allyl phenoxyacetate
ZHANG Jian-hong,TIAN Chui-liang.Synthesis of allyl phenoxyacetate[J].Chemical Engineer,2004,18(8):10-12.
Authors:ZHANG Jian-hong  TIAN Chui-liang
Affiliation:ZHANG Jian-hong1,TIAN Chui-liang2
Abstract:Phenoxyacetic acid was synthesized with phenol and chloroacetic acid as raw material and tetrabutylammonium iodide as catalyst,the yield can reach 96.2%under the optimun conditions.And allyl phenoxacetate was synthesized by esterification of phenoxyacetic acid and allyl alcohol catalyzed by a strong acid cation exchange resin,the yield can reach 91.5%under the optimun conditions.The factors that influence the two reactions were examined.
Keywords:phenoxyacetic acid  allyl alcohol  synthesis  allyl phenoxyacetate
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