| P(AN/VAc)/Clay纳米复合材料的制备及表征 |
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| 引用本文： | 顾晓华,西鹏,李青山,周振芳,倪士民,沈新元.P(AN/VAc)/Clay纳米复合材料的制备及表征[J].高分子材料科学与工程,2006,22(3):235-238. |
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| 作者姓名： | 顾晓华 西鹏 李青山 周振芳 倪士民 沈新元 |
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| 作者单位： | 东华大学材料科学与工程学院,纤维材料改性国家重点实验室,上海,200051;齐齐哈尔大学,黑龙江,齐齐哈尔,161006;东华大学材料科学与工程学院,纤维材料改性国家重点实验室,上海,200051;东华大学材料科学与工程学院,纤维材料改性国家重点实验室,上海,200051;燕山大学亚稳材料制备技术与科学国家重点实验室,河北,秦皇岛,066004 |
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| 基金项目： | 黑龙江省科技厅科技攻关项目;黑龙江省教育厅科学技术研究项目;黑龙江省教育厅科学技术研究项目 |
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| 摘 要： | 通过原位聚合方法制备了聚(丙烯腈-醋酸乙烯酯)/蒙脱土(P(AN/VA c)/C lay)纳米复合材料。通过TEM、X-R ay、IR、NM R、DSC、TG对其形貌、粒径、组成、结晶结构和热性能等进行了表征,结果表明,P(AN/VA c)/C lay纳米复合材料的粒径尺寸为50 nm~80 nm,并呈多片层结构,clay片层均匀分布于P(AN/VA c)基体中,其耐热性均优于P(AN/VA c)。
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| 关 键 词： | 聚(丙烯腈-醋酸乙烯酯)/蒙脱土 纳米 复合材料 |
| 文章编号： | 1000-7555（2006）03-0235-04 |
| 收稿时间： | 2005-03-26 |
| 修稿时间： | 2005-03-262005-06-17 |
PREPARATION AND CHARACTERIZATION OF P(AN/VAc)/CLAY BASED NANO-COMPOSITE |
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| GU Xiao-hua,XI Peng,LI Qing-shan,ZHOU Zhen-fang,NI Shi-min,SHEN Xin-yuan.PREPARATION AND CHARACTERIZATION OF P(AN/VAc)/CLAY BASED NANO-COMPOSITE[J].Polymer Materials Science & Engineering,2006,22(3):235-238. |
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| Authors: | GU Xiao-hua XI Peng LI Qing-shan ZHOU Zhen-fang NI Shi-min SHEN Xin-yuan |
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| Abstract: | P(AN/VAc)/Clay was preparated by in-situ polymerization in this paper.The superficial appearance,particulate dimension,compose,crystallizing structure and hot behavior of the composite were proved through TEM,X-ray,IR,NMR,DSC,TG.The results indicate that the particulate dimension of the nano-composite is 50 nm~80 nm,which belongs to nanometer,and the composite has multi-layer structure.The results also show that intensity,stability of dimension and heat-resistant property of P(AN/VAc)/Clay are all superior to that of P(AN/VAc),which is significative for polyacrylonitrile fiber or acrylic fiber. |
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| Keywords: | P(AN/VAc)/clay nanometer composite material |
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