| 凉味剂薄荷甘油醚的合成研究 |
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| 引用本文： | 马洪亮,吴奇林,李锐,莫东升.凉味剂薄荷甘油醚的合成研究[J].北京轻工业学院学报,2011(3):13-15. |
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| 作者姓名： | 马洪亮 吴奇林 李锐 莫东升 |
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| 作者单位： | 深圳波顿香料有限公司,广东深圳518051 |
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| 摘 要： | 以薄荷脑为起始原料，先与环氧氯丙烷在无水三氯化铝催化作用下，反应制得1-氯-3-薄荷氧基-2-丙醇，然后经酯化、水解反应获得凉味剂薄荷甘油醚．三步反应总得率为71．3％，产品经色质分析证明其结构与薄荷甘油醚相符．该合成方法原料价廉易得、反应得率高、适合工业化生产．
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| 关 键 词： | 薄荷脑 薄荷甘油醚 凉味剂 |
Synthesis of Coolant Agent of Menthol Glyceryl Ether |
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| MA Hong-liang,WU Qi-lin,LI Rui,MO Dong-sheng.Synthesis of Coolant Agent of Menthol Glyceryl Ether[J].Journal of Beijing Institute of Light Industry,2011(3):13-15. |
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| Authors: | MA Hong-liang WU Qi-lin LI Rui MO Dong-sheng |
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| Affiliation: | ( Boton Flavors ＆ Fragrances Co. , Ltd. , Shenzhen 518051, China) |
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| Abstract: | L-Methyl glyceryl ether was synthesized from L-menthol and Epichlorohydrin by three steps. The total yield was 71.3%. The structure of Menthol glyceryl ether obtained was confirmed by GC-MS. This synthetic method had some advantages, such as cheap raw material and high yield, which is suitable for commercial production. |
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| Keywords: | menthol menthol glyceryl ether coolant agent |
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