| 机械合金化制备SbSn金属间化合物的研究 |
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| 引用本文： | 刘晓,曹晶晶,云志,史美仁.机械合金化制备SbSn金属间化合物的研究[J].材料科学与工艺,2006,14(3):305-307. |
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| 作者姓名： | 刘晓 曹晶晶 云志 史美仁 |
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| 作者单位： | 南京工业大学,化学化工学院,江苏,南京,210009;南京工业大学,化学化工学院,江苏,南京,210009;南京工业大学,化学化工学院,江苏,南京,210009;南京工业大学,化学化工学院,江苏,南京,210009 |
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| 摘 要： | 用机械合金化法制备SbSn金属间化合物.使用X射线衍射仪、扫描电子显微镜、透射电镜和DSC差热分析方法对Sb、Sn混合粉末经不同工艺条件合成的产物进行了分析.结果表明:机械合金化法可合成Sb-Sn金属间化合物;随着机械合金化持续进行,合金化的粉末和晶粒不断细化,晶粒内部产生很大的晶格畸变,并且球磨产生的密度和缺陷使原子扩散加快.
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| 关 键 词： | 金属间化合物 机械合金化 Sb Sn |
| 文章编号： | 1005-0299(2006)03-0305-03 |
| 收稿时间： | 2004-02-14 |
| 修稿时间： | 2004年2月14日 |
Study on mechanical alloying of SbSn intermetallic compound |
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| LIU Xiao,CAO Jing-jing,YUN Zhi,SHI Mei-ren.Study on mechanical alloying of SbSn intermetallic compound[J].Materials Science and Technology,2006,14(3):305-307. |
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| Authors: | LIU Xiao CAO Jing-jing YUN Zhi SHI Mei-ren |
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| Affiliation: | College of Chemistry and Chemical Engineering, Nanjing University of Technology, Nanjing 210009, China |
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| Abstract: | The SbSn intermetallic compound was fabricated. Systematic investigations were carried out on the surfacial characteristic and thermal stability of the Sb, Sn milled powders with various milling times using a combination of X - ray powder diffraction, SEM, TEM and differential thermal analysis assisted by DSC. The experimental results show that ball - milling could produce SbSn intermetallic compound in which large lattice distortion was occurred due to the fast diffusion induced by high density of lattice defects. It was found that the grain size and particle size of SbSn decreased with the milling time. |
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| Keywords: | intermetallic compounds mechanical alloying Sb Sn |
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