| 对氯苯甲脒盐酸盐的制备方法 |
| |
| 引用本文： | 赵越,程原.对氯苯甲脒盐酸盐的制备方法[J].精细化工中间体,2008,38(6). |
| |
| 作者姓名： | 赵越 程原 |
| |
| 作者单位： | 中北大学化工与环境学院,山西,太原,030051 |
| |
| 摘 要： | 采用改进的Pinner法--碱催化法,以对氯苯甲腈为原料,经加成、胺化两步反应合成未见文献报道的新脒类化合物对氯苯甲脒盐酸盐。并且两步反应采用一锅烩法,产品总收率达到85%以上。该化合物经IR与熔点测定来确定。
|
| 关 键 词： | 对氯苯甲脒盐酸盐 Pinner法 碱催化 脒盐 加成 胺化 |
Preparation Method of 4-Chlorobenzene-1-carboximidamide Hydrochloride |
| |
| ZHAO Yue,CHENG Yuan.Preparation Method of 4-Chlorobenzene-1-carboximidamide Hydrochloride[J].Fine Chemical Intermediates,2008,38(6). |
| |
| Authors: | ZHAO Yue CHENG Yuan |
| |
| Affiliation: | ZHAO Yue,CHENG Yuan (School of Chemical Engineering , Environment,North University of China,Taiyuan 030051,China) |
| |
| Abstract: | A new amidine compound 4-chlorobenzene -1 -carboximidamide hydrochloride was synthesized from 4- chlorobenzonitrile using the improved Pinner basic catalysis method through addition and amination reaction, and the overall yield of the target product was 85%. The compound was identified by IR and melting point test. |
| |
| Keywords: | 4-chlorobenzene-1-carboximidamide hydrochloride Pinner basic catalysis amidine salts addition amination |
| 本文献已被 CNKI 维普 万方数据 等数据库收录！ |
|
