| β-环糊精与香兰素包合物的制备及其在棉织物上的固着 |
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| 引用本文： | 王春梅,王跃飞,何瑾馨.β-环糊精与香兰素包合物的制备及其在棉织物上的固着[J].产业用纺织品,2009,27(6). |
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| 作者姓名： | 王春梅 王跃飞 何瑾馨 |
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| 作者单位： | 1. 南通大学化学化工学院,南通,226007
2. 东华大学纺织面料技术教育部重点实验室,上海,201620 |
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| 基金项目： | 纺织面料技术教育部重点实验室开放课题基金项目(0705);;江苏省高校自然科学基础研究项目(08KJD540002);;南通市应用研究计划项目(K2008035) |
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| 摘 要： | 研究了β-环糊精与香兰素包合物的制备工艺,用红外光谱和热分析法对包合物进行了表征。通过正交试验对包合工艺进行了优化,得出最佳包合工艺条件是:β-环糊精与香兰素的摩尔比为1∶1,包合温度为50℃,包合时间为2 h。以柠檬酸为交联剂将包合物处理到织物上,优化的整理液配方是:柠檬酸80 g/L,包合物60 g/L,次亚磷酸钠40 g/L,在160℃焙烘3 min。
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| 关 键 词： | β-环糊精 香兰素 包合物 织物整理 |
Preparation of inclusion |
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| Wang Chunmei,Wang Yuefei,He Jinxin.Preparation of inclusion[J].Technical Textiles,2009,27(6). |
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| Authors: | Wang Chunmei Wang Yuefei He Jinxin |
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| Affiliation: | Chemistry Chemical Industry Academy;Nantong University;Key Laboratory of Textile Science & Technology;Ministry of Education;Donghua University |
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| Abstract: | The inclusion methods of vanillin with β-cyclodextrin were studied.The inclusion complexes were cha-racterized by FTIR and DTA.The inclusion process was selected by orthogonal experiment.The optimum condition was established as the molar ratio of vanillin to β-cyclodextrin was 1∶1,with the inclusion temperature at 50℃ for 2 hours.The inclusion complex was grafted onto cotton fiber by CA as a crosslinking agent.The optimum conditions were CA 80 g/L,the inclusion complex 60 g/L,SHP 40 g/L,cured at 160℃ for 3 min. |
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| Keywords: | β-cyclodextrin vanillin complex fabric finish |
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