| 3-取代剑麻皂素的合成 |
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| 引用本文： | 甘春芳,刘亮,林啟福,陆秀莲,崔建国. 3-取代剑麻皂素的合成[J]. 化工技术与开发, 2012, 41(10): 1-3,51 |
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| 作者姓名： | 甘春芳 刘亮 林啟福 陆秀莲 崔建国 |
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| 作者单位： | 广西师范学院化学系,广西南宁,530001 |
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| 基金项目： | 广西自然科学基金，广西教育厅科研项目 |
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| 摘 要： | 剑麻皂素是一种结构特殊的天然化合物,本文从剑麻皂素出发,首先经过Collins试剂氧化,生成3-羰基剑麻皂素,然后在3-位分别引入肟基、腙基和缩胺硫腙基,合成了一些3-取代剑麻皂素化合物,并对合成条件进行了探讨。
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| 关 键 词： | 剑麻皂素 3-取代剑麻皂素 合成 |
Synthesis of 3-Substituted-Tigogenin |
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| GAN Chun-fang,LIU Liang,LIN Qi-fu,CUI Jian-guo. Synthesis of 3-Substituted-Tigogenin[J]. Technology & Development of Chemical Industry, 2012, 41(10): 1-3,51 |
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| Authors: | GAN Chun-fang LIU Liang LIN Qi-fu CUI Jian-guo |
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| Affiliation: | (College of Chemistry and Life Science,Guangxi Teachers Education University,Nanning 530001,China) |
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| Abstract: | Tigogenin was a kind of compound with a special structure. In this paper, tigogenin was oxidated with Corrins reagent and 3-carbonyl-tigogenin. Using hydroxylamine hydrochloride, hydrazine hydrate and thiosemicarbazide as reactive regents, some different 3-substituted tigogenins were obtained. The reaction conditions were discussed. |
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| Keywords: | tigogenin 3-substituted tigogenin synthesis |
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