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| 分子蒸馏/气相色谱-质谱法分析火麻仁精油挥发性成分 | |
| 引用本文： | 李文峰,方国珊,戴 煌,明 建,肖旭霖. 分子蒸馏/气相色谱-质谱法分析火麻仁精油挥发性成分[J]. 中国粮油学报, 2012, 27(8): 113-118 |
| 作者姓名： | 李文峰 方国珊 戴 煌 明 建 肖旭霖 |
| 作者单位： | 1. 陕西师范大学食品工程与营养科学学院,西安,710062 2. 西南大学食品科学学院,重庆,400715 3. 江苏大学食品工程与生物学院,镇江,212013 4. 西南大学食品科学学院,重庆 400715;西南大学食品科学与工程实验教学中心,重庆 400715 |
| 摘 要： | 运用索氏提取法取得火麻仁脂溶性成分,主要考察了不同蒸馏温度对分子蒸馏制备火麻仁精油组分的影响.通过GC - MS分析得出,250℃条件下蒸馏的火麻仁精油分离出136种成分,鉴定出115种挥发性成分,占该火麻仁精油总成分的98.81％,且精油的组分数量随蒸馏温度的增加而增加.其主要物质有:反-1-异丙基-4-甲基环已烷(22.56％)、乙酸(8.43％)、茴香脑(6.50％)、反-3-甲基-6-(1-甲基乙基)环已烯(5.06％)、1-甲基萘(4.36％)、已醛(3.87％)、己酸(2.63％)、萘(2.93％)等物质. |
| 关 键 词： | 火麻仁 分子蒸馏 精油 气相色谱-质谱法 |
| 收稿时间： | 2011-10-29 |
| 修稿时间： | 2012-02-22 |
Analysis of Essential Oil Volatile Composition from Hemp Seed by Molecular Distillation Extraction Combined with GC-MS |
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| Li Wenfeng , Fang Guoshan , Dai Huang , Ming Jian , Xiao Xulin. Analysis of Essential Oil Volatile Composition from Hemp Seed by Molecular Distillation Extraction Combined with GC-MS[J]. Journal of the Chinese Cereals and Oils Association, 2012, 27(8): 113-118 | |
| Authors: | Li Wenfeng Fang Guoshan Dai Huang Ming Jian Xiao Xulin |
| Affiliation: | 1(College of Food Engineering and Nutritional Science,Shanxi Normal University1,Xi′an 710062)(College of Food Science,Southwest University2,Chongqing 400715)(School of Food and Biological Engineering,Jiangsu University3,Zhenjiang 212013)(Food Science and Engineering Experiment Teaching Center,Southwest University4,Chongqing 400715) |
| Abstract: | This experiment studies the lipid solubility of Cannabis sativa L.by SoxhLet Extraction and the influences on different vaporizing temperatures for molecular distillation to make essential oil of Cannabis sativa L.After analyzing the GC-MS,it can get that the distilled Cannabis sativa L.essential oil under 250 ℃ extracts 136 kinds of compound and identifies 115 kinds of volatile components,which represents 98.81% of the total bulk composition of Cannabis sativa L.essential oil and the components number of essential oil is increasing by the increase of temperature.The main substances are:trans-1-Isopropyl-4-Methylcyclohexane(22.56%),Acetic acid(8.43%),Anethol(6.50%),Cyclohexene,3-methyl-6-(1-methylethyl)-,trans-(5.06%),Naphthalene,1-methyl-(4.36%),Hexanoic acid(2.63%),Naphthalene(2.93%). |
| Keywords: | Cannabis sativa L. molecular distillation essential oil GC-MS |
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