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| 碳纳米管上化学镀镍钴磷合金及其表征 | |
| 引用本文： | 何宝临,吴玉程,叶敏,解挺.碳纳米管上化学镀镍钴磷合金及其表征[J].电镀与涂饰,2008,27(9). |
| 作者姓名： | 何宝临 吴玉程 叶敏 解挺 |
| 作者单位： | 1. 合肥工业大学材料学院,安徽,合肥,230009 2. 合肥工业大学材料学院,安徽,合肥,230009;中科院固体物理研究所,安徽,合肥,230031 3. 合肥工业大学摩擦学研究所,安徽,合肥,230009 |
| 基金项目： | 安徽省科研项目，高等学校博士学科点专项科研项目 |
| 摘 要： | 以化学镀的方法在单壁碳纳米管表面沉积了镍钴磷合金,讨论了Co2 与Ni2 的浓度比、镀液温度、pH对沉积速率的影响.当镀液中Co2 与Ni2 的浓度比为1时,沉积速率最大.pH和温度的升高都会使沉积速率增大.采用场发射扫描电镜(FE-SEM)、透射电镜(TEM)、X射线衍射(XRD)和能谱(EDS)对制备的碳纳米管复合材料进行表征.结果表明:热处理会使碳管上的非晶镍钴磷合金镀层转变为晶态,从而提高镀层性能. |
| 关 键 词： | 镍钴磷合金 碳纳米管 化学镀 沉积速率 表征 热处理 |
Electroless nickel-cobalt-phosphorus alloy plating on carbon nanotube and its characterization |
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| HE Bao-lin,WU Yu-cheng,YE Min,XIE Ting.Electroless nickel-cobalt-phosphorus alloy plating on carbon nanotube and its characterization[J].Electroplating & Finishing,2008,27(9). | |
| Authors: | HE Bao-lin WU Yu-cheng YE Min XIE Ting |
| Abstract: | A Ni-Co-P alloy was prepared on the surface of single-wall carbon nanotube by electroless plating.The effects of the concentration ratio of Co2 to Ni2 , bath temperature and pH on deposition rate were discussed.The deposition rate reached a maximum when the concentration ratio of Co2 to Ni2 is 1.The increase of pH and temperature increases the deposition rate.The carbon nanotube composite was characterized by field-emission scanning electron microscopy(SEM), transmission electron microscopy(TEM), X-ray diffraction(XRD) and energy dispersive spectroscopy(EDS).The results showed that the heat treatment induces a transition of Ni-Co-P alloy deposit on carbon nanotube from amorphous to crystalline, resulting in an improvement of deposit properties. |
| Keywords: | nickel-cobalt-phosphorus alloy carbon nanotube electroless plating deposition rate characterization heat treatment |
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