| 溶胶凝胶法制备TiO2薄膜及其润湿性研究 |
| |
| 引用本文： | 贺惠蓉,马养民,胡亚微,杨秀芳. 溶胶凝胶法制备TiO2薄膜及其润湿性研究[J]. 表面技术, 2012, 41(4): 4-6，9 |
| |
| 作者姓名： | 贺惠蓉 马养民 胡亚微 杨秀芳 |
| |
| 作者单位： | 陕西科技大学教育部轻化工助剂与技术重点实验室,西安,710021;陕西科技大学教育部轻化工助剂与技术重点实验室,西安,710021;陕西科技大学教育部轻化工助剂与技术重点实验室,西安,710021;陕西科技大学教育部轻化工助剂与技术重点实验室,西安,710021 |
| |
| 基金项目： | 陕西省自然科学基金(2011JQ2009);陕西省教育厅专项科研计划(11JK0561);陕西科技大学博士科研启动基金(BJ10-22);高等学校博士学科点专项科研基金新教师类资助课题(20116125120004) |
| |
| 摘 要： | 采用溶胶凝胶法,于金属基片上构筑TiO2薄膜,通过修饰1H,1H,2H,2H-十七氟癸基三甲氧基硅烷后,薄膜显示疏水性.对TiO2凝胶的热稳定性进行分析,结果显示,在450℃及以上的温度进行热处理,有机成分可被全部除掉.对所制备薄膜的物相组成和显微结构进行表征,并考察热处理温度对薄膜表面形貌及润湿性能的影响,结果表明,热处理温度为550℃时,疏水性能最好,达到超疏水性.
|
| 关 键 词： | TiO2薄膜 溶胶凝胶法 FAS修饰 润湿性 |
| 收稿时间： | 2012-03-14 |
| 修稿时间： | 2012-08-20 |
Preparation of TiO2 Film by Sol-gel Method and It's Wettability |
| |
| HE Hui-rong,MA Yang-min,HU Ya-wei and YANG Xiu-fang. Preparation of TiO2 Film by Sol-gel Method and It's Wettability[J]. Surface Technology, 2012, 41(4): 4-6，9 |
| |
| Authors: | HE Hui-rong MA Yang-min HU Ya-wei YANG Xiu-fang |
| |
| Affiliation: | (Key Laboratory of Auxiliary Chemistry & Technology for Chemical Industry,Ministry of Education, Shaanxi University of Science & Technology,Xi’an 710021,China) |
| |
| Abstract: | The TiO2 films were prepared on metal substrates by sol-gel method,and showed hydrophobicity after modified with low-surface-energy material 1H,1H,2H,2H-perfluoro-decyltrimethoxysilane(FAS).The heat-stability of TiO2 gel was investigated by thermogravimetric analysis(TG),and the result displayed that the organic matter was completely decomposed when the temperature was no lower than 450 ℃.The morphology,phases and the crystallographic structures of as-prepared films were charactered.The effect of heat-treatment of TiO2 film on morphology and wettability was investigated.The results indicated that the TiO2 film showed superhyphobicity heat-treated at 550 ℃. |
| |
| Keywords: | TiO2 film sol-gel method FAS modification wettability |
| 本文献已被 CNKI 万方数据 等数据库收录！ |
| 点击此处可从《表面技术》浏览原始摘要信息 |
|
点击此处可从《表面技术》下载全文 |
|
