A study on the synthesis of water-soluble Sb2S3 |
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| Authors: | Wei-Dong Xiang Guo-Yuan Ji Jing Wei Yu-Xiang Yang Xiang-Nong Liu |
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| Affiliation: | 1.College of Chemistry and Materials Engineering,Wenzhou University,Wenzhou, Zhejiang,P. R. China;2.Department of Chemistry,East China University of Science and Technology,Shanghai,P. R. China;3.Analysis Test Center,Yangzhou University,Yangzhou,P. R. China |
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| Abstract: | Water-soluble Sb2S3 sub-microspheres were synthesized by aqueous-phase arrested precipitation using mercaptoacetic acid as capping agent and thioacetamide (TAA) as sulfur source. The effects of the experimental conditions, such as temperature, sulfur source, reactants concentration and reaction time, on the shapes, structures and properties of the products were studied. FESEM, TEM showed the products have uniform size distribution. In addition, ultraviolet-visible spectrophotometry (UV-vis) and photoluminescence (PL) showed the resulting products have excellent optical properties. |
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