| 硫代黄色素T的合成 |
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| 引用本文： | 张丽洁,崔军民,惠培华,柳恒,姬明理,张创军. 硫代黄色素T的合成[J]. 陕西化工, 2009, 0(6): 919-920 |
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| 作者姓名： | 张丽洁 崔军民 惠培华 柳恒 姬明理 张创军 |
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| 作者单位： | 西安近代化学研究所,陕西西安710065 |
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| 摘 要： | 研究了以对二甲氨基苯甲酸为原料,通过酰氯化反应,再和5-甲基-2-甲氨基苯硫酚进行缩合反应合成硫代黄色素T。产品的总收率大于75%。
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| 关 键 词： | 对二甲氨基苯甲酸 酰氯化反应 5-甲基-2-甲氨基苯硫酚 缩合反应 黄色素T 合成 |
Synthesis of thioflavine T |
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| ZHANG Li-jie,CUI Jun-min,HUI Pei-hua,LIU Heng,JI Ming-li,ZHANG Chuang-jun. Synthesis of thioflavine T[J]. Applied Chemical Industry, 2009, 0(6): 919-920 |
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| Authors: | ZHANG Li-jie CUI Jun-min HUI Pei-hua LIU Heng JI Ming-li ZHANG Chuang-jun |
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| Affiliation: | ( Xi＇ an Mordern Chemistry Research Institute, Xi＇ an 710065, China) |
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| Abstract: | The synthesis of thioflavine T was studied using p-dimethylaminobenzoic acid as material through chloroformylation reaction, and then by the condensation reaction with 5-methyl-2-methylaminothiophenol. The overall yield of the product was 75%. |
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| Keywords: | p-dimethylaminobenzoic acid chloroformylation reaction 5-methyl-2-methylaminoth-iophenol condensation reaction thioflavine T synthesis |
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