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沉淀转化法回收酸浸渣中铅的酸溶工艺研究
引用本文:张福元,卓俭进,张玉明,彭国敏.沉淀转化法回收酸浸渣中铅的酸溶工艺研究[J].无机盐工业,2013,45(11):47-49.
作者姓名:张福元  卓俭进  张玉明  彭国敏
作者单位:河南中原黄金冶炼厂有限责任公司,河南省黄金资源综合利用重点实验室,河南三门峡 472000
摘    要:以金精矿焙烧-酸浸除杂后的酸浸渣与碳酸氢铵反应生成的转化渣为原料,进行酸溶浸铅工艺研究。通过正交实验考察了液固质量比、浸出pH和浸出时间等因素对铅浸出率的影响,得到最佳工艺条件:浸出液固质量比为2∶1、浸出液pH=0.5、浸出时间为2 h。在此条件下,金属铅浸出率可达83%。

关 键 词:酸浸渣  沉淀转化    硝酸  浸出  

Research on acid leaching process of lead from leaching residue with precipitation transformation method
Zhang Fuyuan;Zhuo Jianjin;Zhang Yuming;Peng Guomin.Research on acid leaching process of lead from leaching residue with precipitation transformation method[J].Inorganic Chemicals Industry,2013,45(11):47-49.
Authors:Zhang Fuyuan;Zhuo Jianjin;Zhang Yuming;Peng Guomin
Affiliation:Henan Key Laboratory of Gold Resources Utilization,Henan Zhongyuan Gold Smelter Co.,Ltd.,Sanmenxia 472000,China
Abstract:With the transformation slag,prepared from the reaction of the refined acid leaching residue from gold concentrate roasting-acid leaching process with ammonium hydrogen carbonate,as the raw material,the acid leaching technology of lead was researched.Through the orthogonal experiment,the influences of various factors,such as liquid/solid mass ratio of leaching solution,pH,and leaching time,on the lead leaching rate were investigated.The optimum process conditions were obtained: liquid/solid mass ratio of leaching solution was 2∶1,pH of leaching solution was 0.5,and leaching time was 2 h.Under those conditions the metal lead leaching rate could reach 83%.
Keywords:acid leaching residue  precipitation transformation  lead  nitric acid  leaching  
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