微波合成离子液体的研究 |
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引用本文: | 洪淑翠. 微波合成离子液体的研究[J]. 山东化工, 2011, 40(10): 22-24 |
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作者姓名: | 洪淑翠 |
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作者单位: | 淄博职业学院化学工程系,山东淄博,255013 |
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基金项目: | 国家重点基础研究发展计划 |
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摘 要: | 在未经改装的家用微波炉中,利用微波间歇辐射的方法,几分钟内制备出多种离子液体。反应时间分别为:[Emim]Br4.5min、[Bmim]Br4.0min、[Emim]BF4 3.5min。结果表明微波加热可显著提高合成速率。[Emim]BF4离子液体的结构经红外光谱验证。
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关 键 词: | 室温离子液体 微波辐射 合成 |
Study on the Microwave - assisted Synthesis of Ionic Liquids |
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Affiliation: | HONG Shu - cui ( Department of Chemical Engineering, Zibo Vocational Institute, Zibo 255013, China) |
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Abstract: | Using microwave intermittence radiation method, prepared several ionic liquids in the microwave ovens without convertion in several minutes. The reaction time was [ Emim] Br 4.5min, [ Bmim] Br 4.0min, [ Emim] BF4 3.5min,respectively. The result indicated that the microwave heating obviously enhaned the synthesis speed. The structure of the [ Emim ] BF4 ionic liquids had been proved by IR. |
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Keywords: | room - temperature ionic liquids microwave radiation synthesis |
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