| 微波促进下9-芳基十氢吖啶衍生物的合成 |
| |
| 引用本文： | 田桂芬,蒯海伟. 微波促进下9-芳基十氢吖啶衍生物的合成[J]. 化工中间体, 2007, 0(11): 13-15,19 |
| |
| 作者姓名： | 田桂芬 蒯海伟 |
| |
| 作者单位： | 淮阴工学院,江苏,淮安,223003 |
| |
| 摘 要： | 以乙醇为溶剂，在高压条件、微波促进下利用芳醛、1，3-环己二酮（CHDO）、醋酸铵为原料一步合成了9-芳基十氢吖啶。整个反应快速高效、绿色环保、后处理简单。产物结构由气相色谱-质谱联用仪（GC／HS）进行分析，经红外光谱及熔点测定确证，并推断了产物可能的合成机理。
|
| 关 键 词： | 9-芳基十氢吖啶 微波促进 高压 医药中间体 |
| 文章编号： | 1006-253x（2007）11-013-3 |
| 收稿时间： | 2007-06-22 |
Synthesis of 9-Aryldecahydroacridine derivatives under Microwave Irradiation |
| |
| TIAN Gui-fen,KUAI Hai-wei. Synthesis of 9-Aryldecahydroacridine derivatives under Microwave Irradiation[J]. , 2007, 0(11): 13-15,19 |
| |
| Authors: | TIAN Gui-fen KUAI Hai-wei |
| |
| Affiliation: | TIAN Gui-fen, KUAI Hai-wei (Huaiyin Istitute of Technology, Huai＇an 223003, Jiangsu, China) |
| |
| Abstract: | Under high pressure and microwave irradiation, a series of 9-aryldecahydroacridine derivatives were synthesized by the reaction of aromatic aldehydes, 1,3-cyclohexanedione and NH4OAc in enthanol. The entire reactions were rapid and efficient. The structures of aim outcomes were analysed by the GC/MS, and corroborated by FTIR and Melting point detector. The he possible mechanism of products was also inferred. |
| |
| Keywords: | 9-aryldecahydroacridine derivatives microwave irradiation high pressure medical Intermediates |
| 本文献已被 维普 万方数据 等数据库收录！ |
|
