| 1-癸烯制备润滑油基础油的合成研究 |
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| 引用本文： | 马建梅,李惠萍,胡子昭,吴浩.1-癸烯制备润滑油基础油的合成研究[J].当代化工,2011,40(6):557-559,564. |
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| 作者姓名： | 马建梅 李惠萍 胡子昭 吴浩 |
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| 作者单位： | 新疆大学化学化工学院,新疆乌鲁木齐,830008 |
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| 摘 要： | 以Al（Et）2Cl/TiCl4为催化剂对1-癸烯齐聚制备润滑油基础油的合成实验进行研究。考察了不同主催化剂、催化剂用量、Al/Ti摩尔比、反应时间和反应温度对PAO的影响。结果表明,以Al（Et）2Cl/TiCl4为催化剂在50℃下反应4 h制备PAO是可行的,并且产物收率高,性能优良。
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| 关 键 词： | 一氯二乙基铝 四氯化钛 1-癸烯 基础油 |
Study on Synthesis of Lube Base Oil by Oligomerization of 1-Decene |
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| MA Jian-mei,LI Hui-ping,HU Zi-zhao,WU-Hao.Study on Synthesis of Lube Base Oil by Oligomerization of 1-Decene[J].Contemporary Chemical Industry,2011,40(6):557-559,564. |
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| Authors: | MA Jian-mei LI Hui-ping HU Zi-zhao WU-Hao |
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| Affiliation: | MA Jian-mei,LI Hui-ping,HU Zi-zhao,WU-Hao(School of Chemistry and Chemical Engineering,Xinjiang University,Xinjiang Urumq 830046,China) |
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| Abstract: | Synthesis of lube base oil from 1-decene over Al（Et）2Cl/TiCl4 catalyst was studied.Effect of catalyst type,catalyst dosage,Al/Ti molar ratio,reaction time and reaction temperature on properties of obtained polymer alpha-olefin（PAO）were investigated.The results show that it is feasible to prepare PAO with Al（Et）2Cl/TiCl4 as catalyst under 50 ℃ for 4 h,yield of oligomer is high and property of product is well. |
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| Keywords: | Chlorodiethyl-aluminum Titanium tetrachloride 1-decene Base oil |
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