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高性能钼棒制备工艺研究
引用本文:杨晓维,李高林,王飞,武宇.高性能钼棒制备工艺研究[J].中国钨业,2014(6):50-52.
作者姓名:杨晓维  李高林  王飞  武宇
作者单位:西安诺博尔稀贵金属材料有限公司,陕西 西安,710210
摘    要:X射线管转轴的高性能钼棒制备是钼材加工中的一个难点,研究选用适宜的钼粉,制定合理烧结工艺,采用特殊的锻造工艺,生产出性能指标达到美国ASTM387-90标准的钼棒。结果表明:采用平均粒度2.2μm,松装密度1.14 g/cm3的钼粉压制后在氢气感应炉中1 920℃烧结3 h后,再采用加热1 2001 400℃,道次加工率24%1 400℃,道次加工率24%2%,总加工率74%,5次模锻的锻造工艺能获得密度为10.2 g/cm3的钼棒,再经900℃保温半小时的消应力退火,可以得到抗拉强度大于620 MPa,延伸率大于30%,组织结构均匀的高性能钼棒。

关 键 词:钼粉  钼棒烧结  锻造  力学性能  抗拉强度  延伸率

Preparation Technology of High Performance Molybdenum Rod System
YANG Xiao-wei,LI Gao-lin,WANG Fei,WU Yu.Preparation Technology of High Performance Molybdenum Rod System[J].China Tungsten Industry,2014(6):50-52.
Authors:YANG Xiao-wei  LI Gao-lin  WANG Fei  WU Yu
Affiliation:(Xi'an Noble Rare and Precious Metal Materials Co. Ltd., Xi'an 710210, Shaanxi, China)
Abstract:Preparation of high-performance X-ray tube molybdenum rod shaft is one of the difficult points of molybdenum processing. Molybdenum rod shaft, whose performance properties conform to US standards ASTM387-90, is produced by sintering and forging processes. Molybdenum powder(average particle size=2.2μm, bulk density=1.14 g/cm3 ) is sintered at 1 920℃for 3 hours in Hydrogen induction furnace. Molybdenum rod (density=10.2 g/cm3) is obtained upon 1200~1400℃heating and 5 times of forging (pass processing rate=24%~2%, total processing rate=74%). High performance molybdenum rod with uniform organizational structure (tensile strength greater than 620MPa, elongation more than 30%) is produced upon Eliminate stress annealing at 900℃for 30 mins.
Keywords:molybdenum powder  molybdenum rod  sintering  forging  mechanical properties  tensile strength  elongation
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