Observations of room-temperature creep recovery in titanium alloys

Conventional α(hcp) and α(hcp)/β(bcc) titanium alloys exhibit significant primary creep strains at room temperature and at stresses well below their macroscopic yield strength. It has been previously reported in various materials systems that repeated unloading during primary creep testing may either accelerate or retard the accumulation of creep strains. These effects have been demonstrated to depend on both microstructure and the applied stress. This article demonstrates that significant room-temperature recovery occurs in technologically relevant titanium alloys. These recovery mechanisms are manifested as a dramatic increase in creep rates (by several orders of magnitude) upon the introduction of individual unloading events, ranging from 1 minute to 365 days, during primary creep tests. Significant increases in both creep rate and the total accumulated creep strain were observed in polycrystalline single α-phase Ti-6Al, polycrystalline α/β Ti-6Al-2Sn-4Zr-2Mo-0.1Si, and individual α/β colonies of Ti-6242. Based on transmission electron microscopy (TEM) studies of the active deformation mechanisms, it is proposed that the presence of significant stress concentrations within the α phase of these materials, in the form of dislocation pileups, is a prerequisite for significant room-temperature recovery. This article is based on a presentation made in the symposium entitled “Defect Properties and Mechanical Behavior of HCP Metals and Alloys” at the TMS Annual Meeting, February 11–15, 2001, in New Orleans, Louisiana, under the auspices of the following ASM committees: Materials Science Critical Technology Sector, Structural Materials Division, Electronic, Magnetic & Photonic Materials Division, Chemistry & Physics of Materials Committee, Joint Nuclear Materials Committee, and Titanium Committee.