| 电化学沉积法制备阿司匹林铜 |
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| 引用本文： | 王鹏,王一雯,纪超男,李琳,王崇臣. 电化学沉积法制备阿司匹林铜[J]. 北京建筑工程学院学报, 2011, 27(3): 28-31 |
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| 作者姓名： | 王鹏 王一雯 纪超男 李琳 王崇臣 |
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| 作者单位： | 北京建筑工程学院环境与能源工程学院,北京,100044 |
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| 基金项目： | 北京市属高等学校人才强教计划资助项目(PHR201008372) |
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| 摘 要： | 以市售阿司匹林药片和铜片（牺牲阳极）为原料,利用电化学沉积法制备了标题化合物,并通过傅立叶变换红外光谱、X-射线衍射及单晶X-射线衍射对其进行表征.讨论了溶液浓度、初始pH、施加电压等条件对产物的影响,确定了最佳合成条件.该法反应装置简单、能避免副产物的产生,产物纯度高,而且是一种绿色合成法.
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| 关 键 词： | 阿司匹林铜 电化学沉积法 单晶 红外光谱 粉末X-射线衍射 单晶X-射线衍射 |
Electro-Chemical Deposition Method to Prepare Copper Aspirin |
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| Wang Peng,Wang Yiwen,Ji Chaonan,Li Lin,Wang Chongchen. Electro-Chemical Deposition Method to Prepare Copper Aspirin[J]. Journal of Beijing Institute of Civil Engineering and Architecture, 2011, 27(3): 28-31 |
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| Authors: | Wang Peng Wang Yiwen Ji Chaonan Li Lin Wang Chongchen |
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| Affiliation: | Wang Peng,Wang Yiwen,Ji Chaonan,Li Lin,Wang Chongchen(School of Environment and Energy Engineering,BUCEA Beijing 100044) |
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| Abstract: | The crystals of the title compounds were prepared by electro-chemical deposition with aspirin tablets and copper piece as precursors,and were characterized by FT-IR,powder X-ray diffraction and single crystal X-ray diffraction respectively.The effects of factors like the initial concentration of aspirin solution,initial pH value on the formation of copper aspirin were also discussed,and the optimum reaction condition was established.The results reveal that electro-chemical deposition is performed with simpl... |
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| Keywords: | copper aspirin electro-chemical deposition infrared spectrum powder X-ray diffraction single crystal X-ray diffraction |
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