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四氯苯酞原药的气相色谱分析
引用本文:徐永,郭利丰.四氯苯酞原药的气相色谱分析[J].现代农药,2012(5):28-29.
作者姓名:徐永  郭利丰
作者单位:浙江省农药检定管理所,杭州 310020
摘    要:介绍了以邻苯二甲酸二正辛酯为内标物,用RXI–17毛细管柱、FID检测器,对四氯苯酞原药进行气相色谱分离和定性、定量分析。采用该方法分析四氯苯酞的线性相关系数为0.9998,变异系数为0.17%,平均回收率为99.7%。该方法操作简便,适用于产品的常规分析和质量控制。

关 键 词:四氯苯酞  气相色谱  分析

Analysis of Phthalide TC by GC
XU Yong,GUO Li-feng.Analysis of Phthalide TC by GC[J].Modern Agrochemicals,2012(5):28-29.
Authors:XU Yong  GUO Li-feng
Affiliation:(Institute for the Control of Agrochemicals of Zhejiang Province,Hangzhou 310020,China)
Abstract:An analysis method for the determination of phthalide TC was developed by GC with RXI–17 capillary column and FID detector using di-n-octyl phthalate as internal standard.The results showed that the linear correlation coefficient was 0.999 8,the variation coefficient was 0.17%,and the average recovery was 99.7%.The method is simple and suitable for routine analysis and quality control of the product.
Keywords:phthalide  GC  analysis
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