| 3,3-二硝基氮杂环丁烷及其复盐的合成 |
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| 引用本文： | 张教强,王伯周,朱春华,龙秋和. 3,3-二硝基氮杂环丁烷及其复盐的合成[J]. 含能材料, 1997, 5(1): 22-25 |
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| 作者姓名： | 张教强 王伯周 朱春华 龙秋和 |
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| 作者单位： | 西安近代化学研究所 |
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| 摘 要： | 采用１－叔丁基－３，３－二硝基氮杂环丁烷为原料，通过苄氧羰基置换叔丁基，通氯化氢脱去苄氧羰基，合成了３，３－二硝基氮杂环丁烷。将ＤＮＡＺ与ＮＴＯ，硝酸，高氯酸和硝仿反应合成了四种复盐，其中ＤＮＡＸ．ＨＣｌＯ４与ＤＮＡＺ．ＨＣｌ（ＮＯ２）３未见文献报道，经元素分析，红外，核磁共振光谱鉴定了化合物结构。
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| 关 键 词： | DNAZ DNAZ复盐 合成 硝基氮杂环丁烷 炸药 |
| 收稿时间： | 1996-07-30 |
SYNTHESIS OF 3,3-DINITROAZETIDINE AND SOME OF ITS COMPLEX SALTS |
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| Zhang Jiao-qiang,Wang Bo-zhou,Zhu Chun-hua and Long Qiu-he. SYNTHESIS OF 3,3-DINITROAZETIDINE AND SOME OF ITS COMPLEX SALTS[J]. Chinese Journal of Energetic Materials, 1997, 5(1): 22-25 |
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| Authors: | Zhang Jiao-qiang Wang Bo-zhou Zhu Chun-hua Long Qiu-he |
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| Abstract: | dinitroazetidine was prepared by treatment of 1 t(butyl) 3,3 dinitroazetidine with benzyl chloroformate and removal of benzyloxy carbonyl from the obtained 1 (benzyloxy carbonyl) 3,3 dinitroazetidine with hydrochloride Four energetic salts of 3,3 dinitroazetidine were prepared by mixing the free base with NTO, HNO 3,HClO 4 and nitroform respectively |
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| Keywords: | dinitroazetidine DNAZ complex salts synthesis |
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