| 气相色谱法测定间苯氧基苯甲醛 |
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| 引用本文： | 李雪辉,朱怀锐,王璐.气相色谱法测定间苯氧基苯甲醛[J].武汉化工学院学报,2012(2):32-33. |
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| 作者姓名： | 李雪辉 朱怀锐 王璐 |
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| 作者单位： | 湖北省蕲农化工有限公司,湖北蕲春435315 |
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| 摘 要： | 为了研究间苯氧基苯甲醛的测定方法,采用了气相色谱面积归一法,使用ov-17石英毛细管柱和氢火焰离子化检测器,柱温230℃,恒温,进样量0.2 uL,对间苯氧基苯甲醛进行分离与定量分析.结果表明：间苯氧基苯甲醛标准偏差为0.042,变异系数为0.042%,平均回收率为99.98%.该方法能满足分析要求,且简单、快速.
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| 关 键 词： | 间苯氧基苯甲醛 气相色谱 面积归一法 定量分析 |
Detection of 3-phenoxybenzaldehyde with GC determination |
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| LI Xue-hui,ZHU Huai-rui,WANG Lu.Detection of 3-phenoxybenzaldehyde with GC determination[J].Journal of Wuhan Institute of Chemical Technology,2012(2):32-33. |
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| Authors: | LI Xue-hui ZHU Huai-rui WANG Lu |
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| Affiliation: | (Qinonghuagong Co.Ltd,Qichun 435315,China) |
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| Abstract: | In order to study GC determination of 3-phenoxybenzaldehyde,a GC area nomalization method was used,with ov-17 quartz capillary column and hydrogen flameionization detector,column temperature of 230 ℃,constant temperature,the injection amount of 0.2 uL,3-phenoxybenzadehyde was sepearated and analyzed quantitively.The results show that standard deviation is 0.042,coefficient of variation is 0.042%,the average recovery rate is 99.98%.The method can meet the requirement of the analysis,and this method is very simple and fast. |
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| Keywords: | 3-phenoxybenzadehyde GC area nomalization method quantitation analysis |
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