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3,3'-二硝基-4,4'一二乙酰氨基二苯醚合成过程中硝化反应的改进
引用本文:付桂云,何旭,刘彩云,徐玉玲,黄斌.3,3'-二硝基-4,4'一二乙酰氨基二苯醚合成过程中硝化反应的改进[J].江西化工,2011(1):108-109.
作者姓名:付桂云  何旭  刘彩云  徐玉玲  黄斌
作者单位:1. 江西师范大学化学与化工学院,江西南昌,330022
2. 宜春职业技术学院,江西宜春,369004
摘    要:3,3'-二硝基-4,4'-二乙酰氨基二苯醚是合成3,3',4,4'-四氨基二苯醚的中间体,本文对其制备过程中的硝化反应进行了改进,获得了较好的效果,并利用FTIR光谱技术对反应产物进行了表征.

关 键 词:3  3'-二硝基-4  4'-二乙酰氨基二苯醚  硝化  改进

Improving nitration in the reaction of 3,3' -dinitro - 4,4' - diacetamido - diphenyl ether
FUGui-yun,HE Xu,LIUCai-yun,XU Yu-ling,HUANG Bin.Improving nitration in the reaction of 3,3' -dinitro - 4,4' - diacetamido - diphenyl ether[J].Jiangxi Chemical Industry,2011(1):108-109.
Authors:FUGui-yun  HE Xu  LIUCai-yun  XU Yu-ling  HUANG Bin
Affiliation:1.Institute of Chemisyry and Chemical Engineering,Jiangxi Normal university 330027;2.Yichun vocational technaical college 369004)
Abstract:3,3'-dinitro-4,4'-diacetamido-diphenyl ether is intermediate in the synthesis of 3,3',4,4'-tetroamino-diphenyl ether 3,3'-dinitro-4,4'-diacetamido-diphenyl ether.In this paper the preparation process of improved nitrification and good results were obtained,and using FTIR spectroscopy characterized of reaction products.
Keywords:3  3'-dinitro-4  4'-diacetamido-diphenyl ether Nitration Improve
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