| 氨基官能化的硅基介孔材料的合成与表征 |
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| 引用本文： | 高文秀,娄大伟,王蕊. 氨基官能化的硅基介孔材料的合成与表征[J]. 吉林化工学院学报, 2012, 29(5): 34-37 |
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| 作者姓名： | 高文秀 娄大伟 王蕊 |
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| 作者单位： | 吉林化工学院化学与制药工程学院,吉林吉林,132022 |
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| 摘 要： | 分别以十六烷基三甲基溴化铵(CTAB)和三嵌段共聚物(P123)为模板剂,正硅酸乙酯(TEOS)为硅源,合成两种硅基介孔材料MCM-41和SBA-15.通过有机硅烷偶连法将3-氨丙基三乙氧基硅烷(APTES)嫁接到已合成的两种介孔材料上,得到氨基官能化的硅基介孔材料.利用XRD、FT-IR、N2吸附-脱附和ICP含量测定对合成的材料进行表征.
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| 关 键 词： | 介孔材料 MCM-41 SBA-15 氨基官能化 |
Synthesis and characterization of amino-functionalized silica-based mesoporous material |
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| GAO Wen-xiu,LOU Da-wei,WANG Rui. Synthesis and characterization of amino-functionalized silica-based mesoporous material[J]. Journal of Jilin Institute of Chemical Technology, 2012, 29(5): 34-37 |
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| Authors: | GAO Wen-xiu LOU Da-wei WANG Rui |
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| Affiliation: | (College of Chemical and Pharmaceutical Engineering,Jilin Institute of Chemical Technology,Jilin City 132022,China) |
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| Abstract: | Silicon-based mesoporous materials MCM-41 and SBA-15 were synthesized with CTAB and P123 as templates and TEOS as silicon source.Through the organic silane coupling method,APTES was grafted onto the synthesized mesoporous materials,which obtains the amino-functionalized silicon-based mesoporous materials.The synthetic materials were characterized by XRD,FI-I,adsorption-desorption for N2 and the determination for ICP content. |
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| Keywords: | hybrid materials MCM-41 SBA-15 amino-functionalized |
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