Electron microscopy and nitrogen adsorption studies of film-type carbon replicas with large pore volume synthesized by using colloidal silica and SBA-15 as templates |
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Authors: | Kamil P Gierszal Chengdu Liang |
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Affiliation: | a Department of Chemistry, Kent State University, Kent, OH 44242, USA b Chemical Sciences Division and Center for Nanophase Materials Sciences, Oak Ridge National Laboratory, Oak Ridge, TN 37831-6201, USA |
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Abstract: | Mesoporous carbons synthesized by the film-type replication of colloidal silica and SBA-15 templates are studied by electron microscopy and nitrogen adsorption. This synthesis strategy involves the formation of thin carbon film on the pore walls of these templates using resorcinol-crotonaldehyde polymer as carbon precursor. For the silica templates consisting of 20-80 nm colloids this synthesis affords carbons with extremely large pore volumes (5-9 cm3/g) and uniform spherical pores reproducing the size of the colloids used. |
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