Preparation of Dark-Red Membrane by Micro-Arc Oxidation on AM50 Alloys |
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Authors: | Z C Shao Q F Zhang L Yang M Wang H Gao |
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Affiliation: | 1. School of Environmental and Chemical Engineering, Shenyang Ligong University, Shenyang, Chinazhongcsh@163.com;3. School of Environmental and Chemical Engineering, Shenyang Ligong University, Shenyang, China |
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Abstract: | The dark-red membrane was prepared on AM50 magnesium alloys by using chemical conversion and micro-arc oxidation (MAO). The effects of MAO electrolyte and chemical conversion solution were researched through L9(34) orthogonal test to obtain formulation for the aforementioned process. Surface morphology, composition, and corrosion resistance were analyzed by X-ray diffraction (XRD), scanning electron microscopy (SEM), and electrochemical test. A dark-red membrane can be obtained by the following steps: first, a chemical conversion was carried out on AM50 alloys by placing them in a solution of 50 g/L KMnO4 and 100 g/L NH4H2PO4 at 50°C for 11 min; second, the prepared alloys were placed into MAO electrolytes containing 10 g/L Na2SiO3 and 5 g/L NaOH in order to obtain the dark-red-colored MAO ceramic membranes. The membranes that are mainly composed of SiO2, MnO, MnP, MgSiO3, and Mg2SiO4 have porous structures. MnO and MnP were identified to be responsible for giving color to the membrane. |
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Keywords: | Alloys Arc Dark Magnesium Micro Oxidation Red |
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