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食用油中痕量镉含量的测定
引用本文:李桂华.食用油中痕量镉含量的测定[J].中国油脂,2004,29(11):61-62.
作者姓名:李桂华
作者单位:烟台师范学院交通学院,264025,山东省烟台市芝罘区世学路186号
摘    要:将食用油灰化处理后,用APDC-DDTC-MIBK体系萃取富集试液中的镉,利用空气-乙炔火焰原子吸收法测定其含量.建立了优化的测定条件,并对可能存在的元素作了干扰实验.结果表明,测定镉的相对标准偏差为1.8%~3.1%,回收率为97.1%~101.5%,结果十分满意.

关 键 词:食用油  原子吸收法  萃取  痕量镉
文章编号:1003-7969(2004)11-0061-02
修稿时间:2004年4月7日

Determination of the trace amount of cadmium in edible oil
LI Gui-hua.Determination of the trace amount of cadmium in edible oil[J].China Oils and Fats,2004,29(11):61-62.
Authors:LI Gui-hua
Abstract:After the cineration of the edible oil,the cadmium in it was extracted by the APDC-DDTC-MIBK system,and the content of cadmium was then tested with air-acetylene flame atomic absorption spectrometry(FAAS).The optimum testing conditions were established and a test for the probably existing interference elements was performed.The relative standard deviation of the test was 1.8% to 3.1%,the respective recovery rate was 97.1% to 101.5%.The result of the test is satisfactory.
Keywords:edible oil  atomic absorption spectrometry  extraction  trace cadmium
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