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Spectroscopic and thermal behavior of ZnHg(SCN)4 |
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| Authors: | X.Q Wang,D XuX.F Cheng,M.K Lü D.R Yuan,J HuangG.W Lu,H.X NingX.L Duan,Z.M WangG.T Lü ,S.G LiY Chen,Y.Q Zhou |
| Affiliation: | a Institute of Crystal Materials, State Key Laboratory of Crystal Materials, Shandong University, Jinan 250100, PR China b College of Environmental Science and Engineering, Institute of Modern Analysis, Shandong University, Jinan 250100, PR China c School of Chemical Engineering, Beijing University of Chemical Technology, Beijing 100029, PR China d Laboratory of Geochemistry and Lithosphere Dynamics, Petroleum University, Dongying 250762, PR China e Institute 53th of China’s Ordnance Industry, Jinan 250031, PR China |
| Abstract: | The synthesis and purification of zinc mercury thiocyanate, ZnHg(SCN)4 (ZMTC), are described. The identity of the synthesized compound was characterized by elemental analysis, X-ray powder diffraction, infrared, Raman, and UV/Vis/NIR transmission spectra. The thermal stability and thermal decomposition of ZMTC crystal were investigated by means of thermogravimetric analysis (TGA) and differential scanning calorimetry (DSC) measurements. The intermediates and final products of the thermal decomposition were identified by X-ray powder diffraction (XRPD). |
| Keywords: | C. Infrared spectroscopy C. Raman spectroscopy C. X-ray diffraction C. Thermogravimetric analysis (TGA) C. Differential scanning calorimetry (DSC) |
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