| 硫酸铁铵催化合成肉桂酸甲酯 |
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| 引用本文： | 俞善信,张鲁西,曾佑林. 硫酸铁铵催化合成肉桂酸甲酯[J]. 应用化工, 1999, 0(4) |
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| 作者姓名： | 俞善信 张鲁西 曾佑林 |
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| 作者单位： | 湖南师范大学化学化工学院!长沙410081 |
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| 摘 要： | 在十二水合硫酸铁铵催化下,由肉桂酸和甲醇发生酯化合成了肉桂酸甲酯,当０．０２ ｍ ｏｌ肉桂酸,０．２０ｍ ｏｌ甲醇和０．０１ ｍ ｏｌ催化剂一起回流７．０ ｈ,产品收率达８７．５％ 。
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| 关 键 词： | 肉桂酸甲酯 硫酸铁铵 合成 催化 |
Catalytic Synthesis of Methyl Cinnamate with Ammonium Ferric Sulfate |
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| Yu Shanxin Zhang Luxi Zeng Youlin. Catalytic Synthesis of Methyl Cinnamate with Ammonium Ferric Sulfate[J]. Applied chemical industry, 1999, 0(4) |
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| Authors: | Yu Shanxin Zhang Luxi Zeng Youlin |
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| Abstract: | The methyl cinnamate was synthesis by the esterification of cinnamic acid and methyl alcohol in presence of ammonium ferric sulfate dodecahydrate NH 4Fe(SO 4) 2·12H 2O. Thus,a mixture of 0.02 mol cinnamic acid,0.20 mol methyl alcohol and 0.01 mol catalyst were heated for 7.0 h at refluxing temperature,the yield was 87.5%. |
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| Keywords: | methyl cinnamate ammonium ferric sulfate synthesis catalysis |
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