| 氯甲酸三氯甲酯法合成DV－菊酰氯 |
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| 引用本文： | 曹顺民,杨一葵,薛兵.氯甲酸三氯甲酯法合成DV－菊酰氯[J].农药,1996(12). |
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| 作者姓名： | 曹顺民 杨一葵 薛兵 |
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| 作者单位： | 扬州化工设计研究所 |
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| 摘 要： | 本文报道了由ＤＶ－菊酸甲酯经皂化、酸化制得ＤＶ－菊酸，然后用氯甲酸三氯甲酯酰氯化合成ＤＶ－菊酰氯，含量达到９４．５％，酰氯化收率达到９６％。
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| 关 键 词： | DV－菊酰氯，合成 |
Synthesis of DV-Chrysanthemyl Chloride from Trichloromethyl Chloroformate |
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| Cao Shunmin,Yang Yikui et al..Synthesis of DV-Chrysanthemyl Chloride from Trichloromethyl Chloroformate[J].Pesticides,1996(12). |
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| Authors: | Cao Shunmin Yang Yikui |
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| Affiliation: | Cao Shunmin;Yang Yikui et al. |
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| Abstract: | A new preparation method of DV-chrysanthemyl chloride was described in this paper.Methyl DV-chrysanthemate via saponification,acidification and then chlorination by trichloromethyl chloroformate to give DV-chrysanthemyl chloride.The purity of the product was 94.5%.and yield of chlorination was 96%. |
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| Keywords: | DV-chrysanthemyl chloride synthesis |
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