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表面活性剂在磷酸锌低热固相合成中的应用
引用本文:邹洪涛,刘吉平,唐文华,苏岳锋,虞振飞. 表面活性剂在磷酸锌低热固相合成中的应用[J]. 无机盐工业, 2006, 38(5): 51-53
作者姓名:邹洪涛  刘吉平  唐文华  苏岳锋  虞振飞
作者单位:1. 北京理工大学材料科学与工程学院,北京,100081;黔南民族师范学院化学与化工系
2. 北京理工大学材料科学与工程学院,北京,100081
3. 北京理工大学材料科学与工程学院,北京,100081;黔东南民族师范专科学校化学系
摘    要:利用低热固相化学反应法开展磷酸锌结构材料合成研究,在不同表面活性剂存在下,以不同锌盐为原料,得到了微米级棒状结构、超细零维球状结构、纳米级空心球状结构及纳米级空心球棒状结构,并应用TEM和SEM等手段对产物结构、形貌和尺度的差异进行了表征。得出可以通过适当的实验设计,找到利用低热固相化学反应法合成磷酸锌特定结构材料的方法的结论。

关 键 词:表面活性剂  磷酸锌  固相化学合成  低热条件
文章编号:1006-4990(2006)05-0051-03
收稿时间:2005-12-29
修稿时间:2005-12-29

Application of surfactant in the synthesis of zinc phosphate by low -temperature solid- state chemical reaction
Zou Hongtao,Liu Jiping,Tang Wenhua,Su Yuefeng,Yu Zhenfei. Application of surfactant in the synthesis of zinc phosphate by low -temperature solid- state chemical reaction[J]. Inorganic Chemicals Industry, 2006, 38(5): 51-53
Authors:Zou Hongtao  Liu Jiping  Tang Wenhua  Su Yuefeng  Yu Zhenfei
Abstract:By means of low - temperature solid - state chemical reaction, the synthesis of zinc phosphate with different structures were studied. With different kinds of surfactant and zinc raw material , bar - shaped micro - structure of zinc phosphate product, super particulate spherical zero - dimensional structure, hollow - spherical nano - structure and hollow bar - shaped nano - structure of zinc phosphate product were gotten. The structures, shapes and yardsticks of the product were characterized by TEM and SEM, etc.. It is concluded that through a series of proper experimental designs, the zinc phosphate with specific structure can be synthesized by low - temperature solid - state chemical reaction.
Keywords:surfactant    zinc phosphoric    solid - state chemical reaction   low - temperature condition
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