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| 分子印迹手性功能单体的合成及红外光谱表征 | |
| 引用本文： | 邢占芬,成洪达,苏立强,王伟华. 分子印迹手性功能单体的合成及红外光谱表征[J]. 化学工程与装备, 2008, 0(10) |
| 作者姓名： | 邢占芬 成洪达 苏立强 王伟华 |
| 作者单位： | 1. 山东万杰医学院,山东,淄博,255213;齐齐哈尔大学,黑龙江,齐齐哈尔,161006 2. 山东万杰医学院,山东,淄博,255213 3. 齐齐哈尔大学,黑龙江,齐齐哈尔,161006 |
| 摘 要： | 本文介绍了分子印迹聚合物手性功能单体(S)-(1-苯乙基)-甲基丙烯酰胺的合成方法,并对产物和中间体甲基丙烯酰氯进行红外光谱表征。将甲基丙烯酰氯与丙烯酰氯、苯甲酰氯红外光谱进行比较,发现1756cm~(-1)、1736cm~(-1)峰是v_(C=O)与878.27cm~(-1)倍频峰之间发生费米共振而产生的双峰。 |
| 关 键 词： | 分子印迹聚合物 功能单体 红外光谱 费米共振 |
The Synthesis end infra-red spectral characterize of methacryloyl chloride |
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| Xing Zhanfen Cheng Hongda Su Liqiang Wang Weihua .Sh,ong Wanjie Medical collage,Zibo ,.Qiqihar University,Qiqihar. The Synthesis end infra-red spectral characterize of methacryloyl chloride[J]. Chemical Engineering & Equipment, 2008, 0(10) | |
| Authors: | Xing Zhanfen Cheng Hongda Su Liqiang Wang Weihua .Sh ong Wanjie Medical collage Zibo .Qiqihar University Qiqihar |
| Affiliation: | Xing Zhanfen~(1,2) Cheng Hongda~(*1) Su Liqiang~2 Wang Weihua~2 1.Sh,ong Wanjie Medical collage,Zibo 255213,2.Qiqihar University,Qiqihar 161006 |
| Abstract: | The synthesis method of(S)-(1-phenylethyl)-methlacrylamide,which is the aschiral functional monomer of molecular imprinted polymer,was described in this paper,and the methacryloyl chloride and(S)-(1-phenylethyl)-methlacrylamide were characterized by infrared spectrum.The infra-red spectrogram of methacryloyl chloride was compared with acryloyl chloride and benzoyl chloride,the result showed that 1765cm~(-1) and 1736cm~(-1) were the double peak produced form Fermi sympathetic vibration between the peak of v_... |
| Keywords: | molecularly imprinted polymer cefchiral functional monomer infra-red spectrum Fermi sympathetic vibration |
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