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氮掺杂制备锐钛矿型纳米TiO2及降解甲基橙的研究
引用本文:王红侠,李新星.氮掺杂制备锐钛矿型纳米TiO2及降解甲基橙的研究[J].广州化工,2014(24):65-67.
作者姓名:王红侠  李新星
作者单位:宿迁学院,江苏 宿迁,223800
基金项目:江苏省教育厅自然科学基金项目(13KJD430004);宿迁学院科研基金(2012ky15)
摘    要:采用溶胶凝胶法制备了氮掺杂TiO2光催化剂。考察了氮的掺杂量、热处理温度对TiO2光催化能力的影响。用XRD、 SEM和紫外-可见光分度计对样品的晶型、形貌和光催化性能进行表征。结果表明氮的掺杂有助于改善TiO2的光催化性能,在灯光照射下5%N-TiO2煅烧温度为450℃时表现出较高的光催化活性和降解甲基橙溶液的能力,在80 min内降解甲基橙溶液达到了98%。

关 键 词:溶胶凝胶法  二氧化钛  光催化  甲基橙

Preparation of Nitrogen-Modified TiO2 Nanoparticle and Its Photocatalytic Activity
WANG Hong-xia , LI Xin-xing.Preparation of Nitrogen-Modified TiO2 Nanoparticle and Its Photocatalytic Activity[J].GuangZhou Chemical Industry and Technology,2014(24):65-67.
Authors:WANG Hong-xia  LI Xin-xing
Affiliation:WANG Hong-xia;LI Xin-xing;Suqian College;
Abstract:A nitrogen -modified TiO2( N-TiO2 ) catalyst was prepared by the sol-gel method. The N-TiO2 samples were characterized by X-ray diffraction, SEM and ultraviolet visible spectrophotometer. The results showed that N-TiO2 had higher photocatalytic activity than not doped TiO2. When N substance in the sample was 5%( molar ratio) and the calcination temperature was 450℃, catalytic activity came to the highest. The percent degradation of methyl orange( MO) was 98% for 5%N-TiO2 under simulated irradiation for 80 min.
Keywords:sol-gel method  titania  photocatalysis  methyl orange
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